HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 21431786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 21431779 | HCID 21431779 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21431786 | HCID 21431786 | — |
Reaction Steps
4-cyclohexylcarbonylphenylacetonitrile (1.5 g.), water (1.5 ml.), concentrated sulphuric acid (1.5 ml.) and acetic acid (1.5 ml.) were heated under reflux for 6 hours, cooled, poured into water and extracted with ether. Removal of the solvent and crystallisation from cyclohexane gave the acid, m.p. 94°-95.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04028404 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-f0bac9bdc3094ef4b917066c8f7467f7 |
| Source note | uspto-grants-1977_06 |