HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl chloride → 4-Methyl-4-(prop-2-en-1-yl)morpholin-4-ium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl chloride | HCID 7850 | — |
| Reactant | 4-Methylmorpholine | HCID 7972 | — |
| Product | 4-Methyl-4-(prop-2-en-1-yl)morpholin-4-ium chloride | HCID 66908141 | — |
Reaction Steps
20.2 grams of N-methyl morpholine was added to 50 grams of allyl chloride. A crystalline solid separated within 2 hours. After 18 days at 25° C. the solid was separated, washed with ethyl acetate, and dried. The product melted at 175°-185° C. with decomposition and contained 100.5% of the theoretical chloride content.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04029658 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-a750ba07b58a4391905bfa1c85f849a5 |
| Source note | uspto-grants-1977_06 |