HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonyl isocyanate → HCID 73793272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonyl isocyanate | HCID 77703 | — |
| Reactant | 1-Methyl-2-(nitromethylidene)imidazolidine | HCID 70250046 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 73793272 | HCID 73793272 | — |
Reaction Steps
A solution of 1.43 g of 1A in 20 ml of methylene chloride was treated with 1.99 g of p-tolylsulfonyl isocyanate at room temperature. After a brief period of exothermicity, the mixture was held at room temperature overnight. The mixture then was diluted with 20 ml of dry ether and filtered to give 1, as a white powder, m.p.: 155°- 157°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04029791 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-10e56aaaa9d1481b8e547b577aaf8584 |
| Source note | uspto-grants-1977_06 |