HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21430436, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | 4-Chloro-3-(morpholine-4-sulfonyl)-benzoic acid | HCID 767900 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21430436 | HCID 21430436 | — |
Reaction Steps
273 Grams of 4-chloro-3-morpholinosulfonylbenzoic acid (1.0 mole) were heated under reflux for 5 hours with 0.5 l of N-methylpiperazine. Subsequently the excess base was completely eliminated in vacuo, the residue was dissolved in 2 l of water, and the pH value of the solution was adjusted to 8 by means of 5N HCl. After standing for 3 days at room temperature, the crystalline precipitate was suction-filtered and was recrystallized from water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04029787 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-2b29b13824ff4be3bd89f4cf767d1e98 |
| Source note | uspto-grants-1977_06 |