HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21430502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | 4-Chloro-3-(pyrrolidine-1-sulfonyl)-benzoic acid | HCID 1070198 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21430502 | HCID 21430502 | — |
Reaction Steps
29.0 Grams of 4-chloro-3-pyrrolidinosulfonylbenzoic acid (0.1 mole) were heated with 50 ml of N-methylpiperazine for 4 hours under reflux. Subsequently the reaction solution was introduced into 0.3 l of water, and the pH value of the mixture was adjusted to 3.0 by means of 5N HCl. After having been allowed to stand over night at room temperature, the precipitate was suction-filtered, recrystallized from water and dried at 100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04029787 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-7d047c9661d5430384a644258e7bc78d |
| Source note | uspto-grants-1977_06 |