1-Methylpiperazine → HCID 21430454, compound

HRID 437174Notes

Reaction equation

HRID 437174 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][C:3]=1[S:11]([N:14]1[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]1)(=[O:13])=[O:12].[CH3:20][N:21]1[CH2:26][CH2:25][NH:24][CH2:23][CH2:22]1>>[ClH:1].[CH3:20][N:21]1[CH2:26][CH2:25][N:24]([C:2]2[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][C:3]=2[S:11]([N:14]2[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]2)(=[O:13])=[O:12])[CH2:23][CH2:22]1

Participants

3

Reactant 2

HCID 531671-MethylpiperazineHCID 7678994-Chloro-3-(1-piperidinylsulfonyl)benzoic acid

Product 1

HCID 21430454HCID 21430454, compound

Procedure

The reaction was carried out in a manner analogous to that of Example 37, using 30.4 g of 4-chloro-3-piperidinosulfonyl benzoic acid (0.1 mole) and 50 ml of N-methylpiperazine.

Sources & evidence

ORD record
ord-33e40f1cb82c4184affc78a55f42f992
Source dataset
uspto-grants-1977_06
Patent number
US04029787

Reaction notes

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