HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyacetonitrile → HCID 21430687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyacetonitrile | HCID 7857 | — |
| Reactant | 3-Nitrobenzenesulfonyl chloride | HCID 8476 | — |
| Product | HCID 21430687 | HCID 21430687 | — |
Reaction Steps
Preparation: The technique of Example 2 is used to react glycolonitrile with m-nitrobenzenesulfonyl chloride. The product is recovered from the reaction mixture by filtration and recrystallized from ethanol. The dried product (45% conversion) is an amber solid, m.p. 66°-69° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04029809 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-37e1a7393f2e4ef3a7dad24bde78bc32 |
| Source note | uspto-grants-1977_06 |