HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21430592, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 21430568 | HCID 21430568 | — |
| Product | HCID 21430592 | HCID 21430592 | — |
Reaction Steps
The title compound as its hydrochloride, m.p. 253° C. (decomp.), was prepared by reduction of the free base of the compound obtained in Example 56 using sodium borohydride. The procedure is that described in Example 53. (Found: C, 69.7; H, 7.5; N, 6.6. C24H30N2O2.HCl requires C, 69.5; H, 7.5; N, 6.75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04029801 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-7339a6bd650c44558a7b5951cd37e511 |
| Source note | uspto-grants-1977_06 |