Methyl fluorosulfate → HCID 86734872, compound

Participants

Reaction Steps

2-ethyl-1-(3H)-isoindolone (1.6 g) was dissolved in dry methylene chloride, and methyl fluorosulfonate (1.2 g) was was added. The reaction mixture was stirred for 30 minutes and then evaporated to dryness. The resuling oil was triturated with acetonitrile and ether. The solid intermediate compound was collected by filtration and used for preparing dyes without further purification.

Provenance & Evidence