HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl Isothiocyanate → 1-[4-(2-Formylhydrazinyl)-3-methoxyphenyl]-3-phenylthiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl Isothiocyanate | HCID 7673 | — |
| Reactant | 1-Formyl-2-(4-amino-2-methoxyphenyl)hydrazine | HCID 21427842 | — |
| Product | 1-[4-(2-Formylhydrazinyl)-3-methoxyphenyl]-3-phenylthiourea | HCID 21427824 | — |
Reaction Steps
Procedure (18.) was employed with 1-formyl-2-(4-amino-2-methoxyphenyl)hydrazine (1.0 g, 0.0056 mole) and phenyl isothiocyanate (0.75 g, 0.0056 mole). Yield 0.90 g (51%), m.p. 183°-184° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04031127 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-6efd904eef3b49aea3c18a457d7bdf3d |
| Source note | uspto-grants-1977_06 |