HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexyl isothiocyanate → 3-Cyclohexyl-1-[4-(2-formylhydrazino)-3-methoxyphenyl]thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexyl isothiocyanate | HCID 14289 | — |
| Reactant | 1-Formyl-2-(4-amino-2-methoxyphenyl)hydrazine | HCID 21427842 | — |
| Product | 3-Cyclohexyl-1-[4-(2-formylhydrazino)-3-methoxyphenyl]thiourea | HCID 21427825 | — |
Reaction Steps
Procedure (11.) was employed with 1-formyl-2-(4-amino-2-methoxyphenyl)hydrazine (1.2 g, 0.0066 mole) and cyclohexyl isothiocyanate (0.93 g, 0.0066 mole). Yield 0.50 g (24%), m.p. 131°-133° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04031127 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-eda235568a5a431ba0b851a140d89fbd |
| Source note | uspto-grants-1977_06 |