HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenyl isothiocyanate → 1-[4-(2-Formylhydrazino)-3-methoxyphenyl]-3-(4-methoxyphenyl)thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenyl isothiocyanate | HCID 75293 | — |
| Reactant | 1-Formyl-2-(4-amino-2-methoxyphenyl)hydrazine | HCID 21427842 | — |
| Product | 1-[4-(2-Formylhydrazino)-3-methoxyphenyl]-3-(4-methoxyphenyl)thiourea | HCID 21427847 | — |
Reaction Steps
Procedure (18.) was employed with 1-formyl-2-(4-amino-2-methoxyphenyl)hydrazine (1.2g, 0.006 mole) and 4-methoxyphenyl isothiocyanate (1.1 g, 0.0066 mole). Yield 1.6 g (70%), m.p. 160°-162° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04031127 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-49c494145d5245c2a7a3ab8cbc19ee90 |
| Source note | uspto-grants-1977_06 |