Propylamine → N,N'-Dipropylurea

HRID 437535Notes

Reaction equation

HRID 437535 reaction equation
[CH2:1]([N:4]=[C:5]=[O:6])[CH2:2][CH3:3].[CH2:7]([NH2:10])[CH2:8][CH3:9]>>[CH2:1]([NH:4][C:5]([NH:10][CH2:7][CH2:8][CH3:9])=[O:6])[CH2:2][CH3:3]

Participants

3

Reactant 2

HCID 7852PropylamineHCID 61033Propyl isocyanate

Product 1

HCID 69343N,N'-DipropylureaYield 98.4%

Procedure

1700 g. (98.4%) of product was prepared according to the method of Hayes et al., J. Agr. Food Chem. 17, 1077 (1969) from n-propylisocyanate (1020 g. 12 mole) and n-propylamine (708 g., 4.75 mole).

Sources & evidence

ORD record
ord-09f416548e48447692257096144ab4da
Source dataset
uspto-grants-1977_06
Patent number
US04031218

Reaction notes

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