HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21428729, compound → 3-(4-Methylphenoxy)piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21428729 | HCID 21428729 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(4-Methylphenoxy)piperidine | HCID 21428718 | — |
Reaction Steps
A solution of 2.9 g of 1-benzyl-3-(p-tolyloxy) piperidine in 30 ml. of 95% ethanol is added to 0.42 g of 10% Pd-C, and hydrogenated at about 50° C. for 3 hours. Then the reaction mixture is cooled to ambient temperature, the 10% Pd-C is filtered off, and the ethanol is removed leaving a yellow oil of 3-(p-tolyloxy)piperidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04031221 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-bcc6ccc6d8834f7590a0d0ef152c2668 |
| Source note | uspto-grants-1977_06 |