HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 21428712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | 1-(1H-Indol-3-yl)-2-(4-phenoxy-1-piperidinyl)-1,2-ethanedione | HCID 21428692 | — |
| Product | HCID 21428712 | HCID 21428712 | — |
Reaction Steps
By following the manipulative procedure described in Example 4(c), 5.0 g of 1-(indol-3-ylglyoxyloyl)-4-phenoxypiperidine are reacted with 2.8 g of lithium aluminum hydride to give white flakes of 3-[2-(4-phenoxypiperidyl)ethyl]indole, m.p. 123°-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04031221 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-ee90d9a277af4b288f3daebdb1836dd5 |
| Source note | uspto-grants-1977_06 |