HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromohexane → HCID 21428688, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromohexane | HCID 8101 | — |
| Reactant | Fumarate | HCID 5460307 | — |
| Reactant | AR 03 Cl | HCID 6454458 | — |
| Product | HCID 21428688 | HCID 21428688 | — |
Reaction Steps
N,N-Bis-[3-(3,4-dihydro-4,4-dimethyl-1,3-dioxo-2(1H)-isoquinolyl)-propyl]-n-hexylamine was prepared analogous to Example 27 from 2.6 gm of N,N-bis-[3-(3,4-dihydro-4,4-dimethyl-1,3-dioxo-2(1H)-isoquinolyl)-propyl]-amine and 1 gm of n-hexyl bromide. M.p. of the fumarate: 137°-138° C; yield: 1.7 gm (50% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04031219 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-c487c80e30924ff7b23fab91768c2bb6 |
| Source note | uspto-grants-1977_06 |