HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl [4-(Benzyloxy)phenoxy]acetate → Ethyl 2-(4-hydroxyphenoxy)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl [4-(Benzyloxy)phenoxy]acetate | HCID 734886 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 2-(4-hydroxyphenoxy)acetate | HCID 13187337 | — |
Reaction Steps
EThyl 4-benzyloxyphenoxyacetate (5.8 g.) was hydrogenated in the presence of 0.5 g. of palladium-on-carbon catalyst in 200 ml. of absolute ethanol. There was obtained 4.00 g. of ethyl 4-hydroxyphenoxyacetate, m.p. 124°-125° C. when recrystallized from isopropyl alcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04031246 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-484cb848ac3c41708af8cb88f881b814 |
| Source note | uspto-grants-1977_06 |