HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-1-propanol → 3-{4-[2-Chloro10,11-dihydro-dibenz[b,f]oxepin-10-yl]-1-piperazinyl}-1-propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-1-propanol | HCID 12313 | — |
| Reactant | 1-[2-Chloro-10,11-dihydro-dibenz[b,f]oxepin-10-yl]-piperazine | HCID 22767943 | — |
| Product | 3-{4-[2-Chloro10,11-dihydro-dibenz[b,f]oxepin-10-yl]-1-piperazinyl}-1-propanol | HCID 20315124 | — |
Reaction Steps
In an analogous manner to that described in Example 5, from 1-[2-chloro-10,11-dihydro-dibenz[b,f]oxepin-10-yl]-piperazine and 3-chloro-1-propanol, there is obtained 3-{4-[2-chloro10,11-dihydro-dibenz[b,f]oxepin-10-yl]-1-piperazinyl}-1-propanol as an oil. The dihydrochloride, prepared in ethanol, melts at 206°-207° C. (with decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04032525 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-9c9a5bcc842c4d35a8608f495544ab0b |
| Source note | uspto-grants-1977_06 |