HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 20371581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | HCID 20371582 | HCID 20371582 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20371581 | HCID 20371581 | 91% |
Reaction Steps
2 g of α-(3,4-dimethoxyphenethylaminomethyl)-3-benzyloxybenzylalcohol hydrochloride, 0.5 g of 10 % palladium-carbon, 100 ml of isopropanol and 15 ml of water are treated in the same manner as described in Example 1-(c). 1.45 g of α-(3,4dimethoxyphenethylaminomethyl)-3-hydroxybenzylalcohol hydrochloride are obtained. M.p. 161° -162° C.(recrystallized from a mixture of isopropanol and ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04032575 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-c62f13db34d949398f5b65cea7c1c23a |
| Source note | uspto-grants-1977_06 |