HCID 20371578, compound → HCID 20434099, compound

Participants

Reaction Steps

One g of α-(3,4-dimethoxyphenethylaminomethyl)-2-benzyloxybenzylalcohol hydrochloride, 0.3 g of 10 % palladium-carbon and 30 ml of 80 % aqueous isopropanol are treated in the same manner as described in Example 1-(c). 0.75 g of α-(3,4-dimethoxyphenethylaminomethyl)-2-hydroxybenzylalcohol hydrochloride are obtained. M.p. 141° - 143° C.(decomp.)(recrystallized from a mixture of ethanol and ether). 1/2 Oxalate: M.p. 175° -176° C.(recrystallized from ethanol).

Provenance & Evidence