HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 54044653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | L-Glutamic Acid | HCID 33032 | — |
| Reactant | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| Catalyst | Nickel | HCID 935 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 54044653 | HCID 54044653 | — |
Reaction Steps
The product was made from D-glucose and L-(+)-glutamic acid using Raney nickel or palladium/activated carbon (10%) as a catalyst. The product had a melting point of 94° C. and an RF -value of 0.61 (determined on DC-finished plates of silica gel G (Merck) with a transporting fluid made up of 85 parts by volume of methanol and 15 parts by volume of water).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04032676 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-4eb0997309fe4736bea4767a9e210335 |
| Source note | uspto-grants-1977_06 |