HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobenzoic Acid → HCID 21427706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobenzoic Acid | HCID 978 | — |
| Reactant | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | HCID 21427706 | HCID 21427706 | — |
Reaction Steps
As starting materials D-glucose and p-amino-benzoic acid were used. The reductive amination was carried out using Raney nickel as catalyst and heating for 2 hours to 50° C. and for 3 hours to 70° C. The product obtained had a melting point of 111° to 112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04032676 |
| Source dataset | uspto-grants-1977_06 |
| ORD ID | ord-0f24c802f0804449a26f33f75999df83 |
| Source note | uspto-grants-1977_06 |