HRID439312

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=C(O)c1ccc([N+](=O)[O-])c([N+](=O)[O-])c1

HCID10709

Benzoic acid, 3,4-dinitro-

C7H4N2O6

HCID24386

Thionyl chloride

Cl2OS

PRODUCTS

生成物

结构：O=C(Cl)c1ccc([N+](=O)[O-])c([N+](=O)[O-])c1

HCID11806491

3,4-dinitrobenzoyl Chloride

C7H3ClN2O5

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID241

Benzene

C6H6

溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

Typically, the 3,4-dinitrobenzoic acid starting material is dissolved in an aprotic solvent such as benzene or toluene and refluxed with thionylchloride for a period of about 2-6 hours to form the desired 3,4-dinitrobenzoyl chloride.