HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dinitrobenzoic acid → 3,4-dinitrobenzoyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dinitrobenzoic acid | HCID 10709 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Solvent | Benzene | HCID 241 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 3,4-dinitrobenzoyl Chloride | HCID 11806491 | — |
Reaction Steps
Typically, the 3,4-dinitrobenzoic acid starting material is dissolved in an aprotic solvent such as benzene or toluene and refluxed with thionylchloride for a period of about 2-6 hours to form the desired 3,4-dinitrobenzoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05514676 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-bf865068f77d44af88b2f116c9ac3d83 |
| Source note | uspto-grants-1996_05 |