HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 439317Generated: October 31, 2026
Hydrochloric Acid → HCID 22411254, compound
https://huagongshe.com/reaction/439317
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 22411216 | HCID 22411216 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22411254 | HCID 22411254 | 57% |
Reaction Steps
The resultant ester was dissolved in minimum amount of methanol and cooled to 0° C. Dry hydrogen chloride gas was passed through the mixture for 15 minutes. After storing -20° C. overnight, the separated solid was filtered and dried. It was crystallized from ethanol, water and ether to give the desired compound 1.80 g (57%), m.p. 251-252.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05514676 |
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| Source dataset | uspto-grants-1996_05 |
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| ORD ID | ord-e1dbf669f1264511ad4cf8a0adc706d8 |
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| Source note | uspto-grants-1996_05 |
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