Hydrochloric Acid → HCID 22411275, compound

Participants

Reaction Conditions

Reaction Steps

The ester was dissolved in minimum amount of methanol and cooled to 0° C. Dry hydrogen chloride gas was passed through the mixture for 15 minutes. It was stored at -20 ° C. overnight, whereupon the solid which separated was filtered and dried. It was crystallized from ethanol, water and ether mixture to give 1.66 g of the title product (53%), m.p. 247°-249° C.

Provenance & Evidence