HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → HCID 22616257, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | 4-Chloro-3-methyl-1,2-oxazol-5-amine | HCID 10582822 | — |
| Product | HCID 22616257 | HCID 22616257 | 84% |
Reaction Steps
N-(4-Chloro-3-methyl-5-isoxazolyl)benzenesulfonamide was prepared according to the method in Example 1b from 5-amino-4-chloro-3-methylisoxazole and benzenesuIfonyl chloride in 84% yield. The crude product was purified by recrystallization using hexanes/ethyl acetate, m.p. 140°-143° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05514691 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-73e8996cdf724483978362e736bf221b |
| Source note | uspto-grants-1996_05 |