HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → HCID 10784030, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | HCID 10584549 | HCID 10584549 | — |
| Product | HCID 10784030 | HCID 10784030 | 85% |
Reaction Steps
N-(4-Methoxycarbonyl-3-trifluoromethyl-5-isoxazolyl)benzenesulfonamide was prepared as described in Example 25 from 5-amino-4-methoxycarbonyl-3-trifluoromethylisoxazole and benzenesulfonyl chloride in 85% yield. The crude product was purified by recrystallization from methanol/water to give a solid, m.p. 100°-101° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05514691 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-31154794d8d3437389e6f76553e40f99 |
| Source note | uspto-grants-1996_05 |