関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 4-(Phenylmethyl)benzenemethanol | HCID 597614 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | Benzene, 1-(chloromethyl)-4-(phenylmethyl)- | HCID 84334 | — |
反応手順
4-benzylbenzyl alcohol (181.47 g) was dissolved into chloroform (100 ml), and thionyl chloride (66.8 ml) was added with stirring at a 0° C. After stirring at 0° C. for 4 hours, reaction mixture was concentrated under reduced pressure to give the title compound (198.34 g). This product was used in the subsequent procedure without purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05516777 |
|---|
| 出典データセット | uspto-grants-1996_05 |
|---|
| ORD ID | ord-398b48610b59430bad1b318ae6ff4a76 |
|---|
| 出典メモ | uspto-grants-1996_05 |
|---|
