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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 43980Generated: October 29, 2026

HCID 86648860, compound → Ammonium formate

https://huagongshe.com/reaction/43980

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86648860HCID 86648860—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductAmmonium formateHCID 27239232,033.3%
ProductHCID 86648859HCID 86648859—

Reaction Steps

The same operation as in Example (90d) was performed using methyl cis(±)-3-(4-{benzyl[(benzyloxy)carbonyl]amino}-3-methoxypiperidin-1-yl)-2-fluorobenzoate obtained in Example (263a) (31 mg, 0.06 mmol), a 10% palladium-carbon catalyst (20 mg), ammonium formate (39 mg, 0.61 mmol) and methanol (4 mL), to obtain the title compound. The resulting compound was used for the next reaction without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08536197B2
Source datasetuspto-grants-2013_09
ORD IDord-3537a2e10a1048d4af5359289dc523a9
Source noteuspto-grants-2013_09