HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86648860, compound → Ammonium formate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86648860 | HCID 86648860 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ammonium formate | HCID 2723923 | 2,033.3% |
| Product | HCID 86648859 | HCID 86648859 | — |
Reaction Steps
The same operation as in Example (90d) was performed using methyl cis(±)-3-(4-{benzyl[(benzyloxy)carbonyl]amino}-3-methoxypiperidin-1-yl)-2-fluorobenzoate obtained in Example (263a) (31 mg, 0.06 mmol), a 10% palladium-carbon catalyst (20 mg), ammonium formate (39 mg, 0.61 mmol) and methanol (4 mL), to obtain the title compound. The resulting compound was used for the next reaction without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536197B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-3537a2e10a1048d4af5359289dc523a9 |
| Source note | uspto-grants-2013_09 |