HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 178454090, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 178445577 | HCID 178445577 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178454090 | HCID 178454090 | — |
Reaction Steps
Analogously to Example 6b, starting from a solution of 13.2 g (0.03842 mol) of trans3-(N-BOC-amino)-1-(thexyl-dimethylsilyl)oxymethyl-cyclobutane (cf. Example 6c) in 60 ml of tetrahydrofuran and 76.8 ml (0.0768 mol) of a 1M tetrabutylammonium fluoride solution in tetrahydrofuran, the title compound is obtained, m.p. 98°-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05516806 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-23cbff4542244290931430315f79c071 |
| Source note | uspto-grants-1996_05 |