Hydrochloric Acid → HCID 22408684, compound

HRID 439889Notes

Reaction equation

HRID 439889 reaction equation
C([NH:8][CH:9]1[CH2:12][CH:11]([CH2:13][O:14][N:15]2C(=O)C3C(=CC=CC=3)C2=O)[CH2:10]1)(OC(C)(C)C)=O.[ClH:26]>O>[ClH:26].[ClH:26].[NH2:15][O:14][CH2:13][CH:11]1[CH2:12][CH:9]([NH2:8])[CH2:10]1

Participants

4

Procedure

Analogously to Example 6, starting from 1.15 g (0.00332 mol) of 2-[3-(N-BOC-amino)cyclobutylmethoxy]-1H-isoindole-1,3(2H)-dione, 6 ml of water and 5 ml of concentrated hydrochloric acid, the title compound is obtained, m.p. 179° C. (decomp.).

Sources & evidence

ORD record
ord-0651039e0e624d87abc42f45dd075b9f
Source dataset
uspto-grants-1996_05
Patent number
US05516806

Reaction notes

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