HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 6-(5-Indanylamino)-2-thiouracil
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Indan-5-amine | HCID 90496 | — |
| Reactant | 6-Amino-2-thiouracil | HCID 1201441 | — |
| Product | 6-(5-Indanylamino)-2-thiouracil | HCID 22409111 | 6% |
Reaction Steps
6-Amino-2-thiouracil is heated for 4 hours at 160° C. with an equimolar mixture of 5-aminoindan and the hydrochloride of 5-aminoindan. The product is crystallized from ethanol/water and isolated in 6% yield, mp 269°-272° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05516905 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-27542d99fbea424f99c8348047877e08 |
| Source note | uspto-grants-1996_05 |