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HRID439908

反应详情

EQUATION

反应方程式

HRID 439908 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：Nc1ccc2c(c1)CCC2
HCID90496

Indan-5-amine

C9H11N

2 次

结构：Nc1cc(=O)[nH]c(=S)[nH]1
HCID1201441

6-Aminothiouracil

C4H5N3OS

PRODUCTS

生成物

1
结构：O=c1cc(Nc2ccc3c(c2)CCC3)[nH]c(=S)[nH]1
HCID22409111

未命名化合物

收率 6%

PROCEDURE

实验过程

6-Amino-2-thiouracil is heated for 4 hours at 160° C. with an equimolar mixture of 5-aminoindan and the hydrochloride of 5-aminoindan. The product is crystallized from ethanol/water and isolated in 6% yield, mp 269°-272° C.

WORKUP

后处理

  1. customThe product is crystallized from ethanol/water
  2. customisolated in 6% yield, mp 269°-272° C.