HuagongsheHuagongshe Chemistry Print Report · For research reference only
((4-(tert-Butyl)phenyl)ethynyl)trimethylsilane → Trimethylsilyl[4-(4-methylpentyl)]phenylethyne
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ((4-(tert-Butyl)phenyl)ethynyl)trimethylsilane | HCID 14989664 | — |
| Reactant | 4-(4-Methylpentyl)bromobenzene | HCID 22409093 | — |
| Product | Trimethylsilyl[4-(4-methylpentyl)]phenylethyne | HCID 54327813 | — |
Reaction Steps
Using the same general procedure as described for Compound 21, but using instead 4-(4-methylpentyl)bromobenzene (Compound 30), the title compound was synthesized as a colorless oil. PMR (CDCl3): & 0.32 (9H, s), 0.93 (6H, d, J-6.6 Hz), 1.18-1.29 (2H, m), 1.52-1.70 (3H, m), 2.58 (2H, t, J-7.7 Hz), 7.12 (2H, d, J-8.1 Hz), 7.43 (2H, d, J-8.1 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05516904 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-6530a09d05024e3ba8c72547979e750b |
| Source note | uspto-grants-1996_05 |