HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 22077247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Pentyl nitrite | HCID 10026 | — |
| Reactant | 2,4-Dichloro-5-fluoroaniline | HCID 2758098 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22077247 | HCID 22077247 | — |
Reaction Steps
36.0 g (0.20 mol) of 2,4-dichloro-5-fluoroaniline are dissolved at room temperature in 180 ml of ethanol and 36.0 g of concentrated sulfuric acid are added with cooling. To this mixture are added dropwise 27.0 ml (0.23 mol) of amyl 1 nitrite. The diazonium salt precipitated out is then removed by suction and washed with a little diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05516932 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-9a2a7d0e1ae9476bbf2ca0cecb42574d |
| Source note | uspto-grants-1996_05 |