HRID440249

反应详情

EQUATION

反应方程式

HRID 440249 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In 100 ml of methanol was dissolved 1.98 g (0.0068 mole) of 1-t-butoxycarbonyl-3-methoxy-4-phenylaminopyrrolidine obtained as described above, and 23.5 ml of 6N hydrochloric acid was added thereto. The mixture was left to stand at room temperature overnight. The solvent was removed under reduced pressure, and the residue was washed with ethanol to obtain 1.71 g of 3-methoxy-4-phenylaminopyrrolidine hydrochloride as white powder.

WORKUP

后处理

  1. customobtained
  2. additionwas added
  3. waitThe mixture was left
  4. customThe solvent was removed under reduced pressure
  5. washthe residue was washed with ethanol