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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 440249Erstellt: 25. Oktober 2026

Hydrochloric Acid → 3-Methoxy-4-phenylaminopyrrolidine hydrochloride

https://huagongshe.com/reaction/440249

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrochloric AcidHCID 313—
Edukt1-t-Butoxycarbonyl-3-methoxy-4-phenylaminopyrrolidineHCID 21473342—
LösungsmittelMethanolHCID 887—
Produkt3-Methoxy-4-phenylaminopyrrolidine hydrochlorideHCID 21473354—

Reaktionsschritte

In 100 ml of methanol was dissolved 1.98 g (0.0068 mole) of 1-t-butoxycarbonyl-3-methoxy-4-phenylaminopyrrolidine obtained as described above, and 23.5 ml of 6N hydrochloric acid was added thereto. The mixture was left to stand at room temperature overnight. The solvent was removed under reduced pressure, and the residue was washed with ethanol to obtain 1.71 g of 3-methoxy-4-phenylaminopyrrolidine hydrochloride as white powder.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05519016
Quelldatensatzuspto-grants-1996_05
ORD IDord-777e9efddb904059b9ce049d57098e4f
Quellennotizuspto-grants-1996_05