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HRID440500

反应详情

EQUATION

反应方程式

HRID 440500 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：COc1ccccc1C1(C(=O)O)CC1
HCID18400011

1-(2-Methoxyphenyl)cyclopropane-1-carboxylic acid

C11H12O3

PRODUCTS

生成物

1
结构：COc1ccccc1C1(C(=O)Cl)CC1
HCID24273791

未命名化合物

PROCEDURE

实验过程

1-(2-methoxyphenyl)cyclopropane carboxylic acid (19 g) and thionyl chloride (30 ml) were heated under gentle reflux for 2 hours. The solvent was evaporated to yield 1-(2-methoxyphenyl)cyclopropane carbonyl chloride.

WORKUP

后处理

  1. temperatureunder gentle reflux for 2 hours
  2. customThe solvent was evaporated