HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 1-(2-Methoxyphenyl)cyclopropane-1-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1-(2-Methoxyphenyl)cyclopropane-1-carboxylic acid | HCID 18400011 | — |
| Product | 1-(2-Methoxyphenyl)cyclopropane-1-carbonyl chloride | HCID 24273791 | — |
Reaction Steps
1-(2-methoxyphenyl)cyclopropane carboxylic acid (19 g) and thionyl chloride (30 ml) were heated under gentle reflux for 2 hours. The solvent was evaporated to yield 1-(2-methoxyphenyl)cyclopropane carbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05519034 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-9bd963ed53c64b00944548ac86d2f391 |
| Source note | uspto-grants-1996_05 |