HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 86749507, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2-Ethylhexylamine | HCID 7719 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 2-(4-Camphylidenemethylene-anilino)-4,6-dichloro-1,3,5-triazine | HCID 86749508 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86749507 | HCID 86749507 | — |
Reaction Steps
A reaction mixture comprising 33 g (0.26 mol) of 2-ethylhexylamine and 50 g (0.12 mol) of 2-(4-camphylidenemethylene-anilino)-4,6-dichloro-1,3,5-triazine in toluene is heated to 90° C. in the presence of sodium acetate. When the starting materials have reacted completely, the mixture is worked up. The product (95%) is a yellow viscous oil. UV (ethanol, c=1 mg/100 ml): λmax =345 nm, E=0.57.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05520906 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-421b47c7408749a68881a84dac61fe1d |
| Source note | uspto-grants-1996_05 |