Sodium ethoxide → HCID 88201550, compound

HRID 440628Notes

Reaction equation

[C:1]12([CH3:43])[C:7]([CH3:9])([CH3:8])[CH:4]([CH2:5][CH2:6]1)[CH2:3][C:2]2=[C:10]=[C:11]1[CH:42]=[CH:41][C:14]([NH:15][C:16]2[N:21]=[C:20]([NH:22][C:23]3[CH:28]=[CH:27][C:26](=[C:29]=[C:30]4[CH2:35][CH:34]5[C:36]([CH3:38])([CH3:37])[C:31]4([CH3:39])[CH2:32][CH2:33]5)[CH2:25][CH:24]=3)[N:19]=[C:18](Cl)[N:17]=2)=[CH:13][CH2:12]1.[CH2:44]([O-:46])[CH3:45].[Na+]>>[C:1]12([CH3:43])[C:7]([CH3:9])([CH3:8])[CH:4]([CH2:5][CH2:6]1)[CH2:3][C:2]2=[C:10]=[C:11]1[CH:42]=[CH:41][C:14]([NH:15][C:16]2[N:21]=[C:20]([NH:22][C:23]3[CH:28]=[CH:27][C:26](=[C:29]=[C:30]4[CH2:35][CH:34]5[C:36]([CH3:38])([CH3:37])[C:31]4([CH3:39])[CH2:32][CH2:33]5)[CH2:25][CH:24]=3)[N:19]=[C:18]([O:46][CH2:44][CH3:45])[N:17]=2)=[CH:13][CH2:12]1

Participants

Reactant 2

HCID 2723922Sodium ethoxide

HCID 88202079HCID 88202079, compound

Product 1

HCID 88201550HCID 88201550, compound

Procedure

2,4-Bis(4-camphylidenemethylene-anilino)-6-chloro-1,3,5-triazine is reacted with sodium ethanolate analogously to the instructions of Example 2. The desired product forms to the extent of 43%.

Sources & evidence

ORD record: ord-a5e017cb7d624c6e980d124de740e7ed
Source dataset: uspto-grants-1996_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05520906

Reaction notes

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