HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → (Z)-Benzaldehyde oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (Z)-Benzaldehyde oxime | HCID 12143 | 99.2% |
Reaction Steps
10.6 g of benzaldehyde, 7.0 g of hydroxylamine hydrochloride and 14.0 g of sodium carbonate were added to 200 ml of methanol and then stirred for 5 hours at normal temperature. The reaction mixture was filtered and then methanol was distilled off under reduced pressure from the filtrate to obtain 12.0 g (Yield 99%) of the title compound (III-1) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05521146 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-233482af162442449f455612d09bae50 |
| Source note | uspto-grants-1996_05 |