HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Nitrobenzofuran-3(2H)-one → 7-Amino-2,3-dihydro-3-benzofuranone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Nitrobenzofuran-3(2H)-one | HCID 22404759 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | 7-Amino-2,3-dihydro-3-benzofuranone | HCID 22404803 | — |
Reaction Steps
By the method of Example 1, Step E, 2.51 g (0.014 mole) of 2,3-dihydro-7-nitro-3-benzofuranone is reacted with 3.1 g (0.056 mole) of powdered iron in 45 mL of glacial acetic acid and 8 mL of water, yielding 7-amino-2,3-dihydro-3-benzofuranone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05521147 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-6bbcd3de47fa4104a578b6032fb06ea1 |
| Source note | uspto-grants-1996_05 |