Methylamine → HCID 69228727, compound

HRID 440851Notes

Reaction equation

HRID 440851 reaction equation
[CH2:1]([C:4]1[N:8]([CH2:9][C:10]2[CH:15]=[CH:14][C:13]([C:16]3[C:17]([C:22]([O:24][C:25]([CH3:28])([CH3:27])[CH3:26])=[O:23])=[CH:18][CH:19]=[CH:20][CH:21]=3)=[CH:12][CH:11]=2)[C:7]2[CH:29]=[C:30]([N:34]3C(=O)C4=CC=CC=C4C3=O)[CH:31]=[C:32]([CH3:33])[C:6]=2[N:5]=1)[CH2:2][CH3:3].CN>>[CH2:1]([C:4]1[N:8]([CH2:9][C:10]2[CH:15]=[CH:14][C:13]([C:16]3[C:17]([C:22]([O:24][C:25]([CH3:27])([CH3:28])[CH3:26])=[O:23])=[CH:18][CH:19]=[CH:20][CH:21]=3)=[CH:12][CH:11]=2)[C:7]2[CH:29]=[C:30]([NH2:34])[CH:31]=[C:32]([CH3:33])[C:6]=2[N:5]=1)[CH2:2][CH3:3]

Participants

3

Reactant 2

HCID 6329MethylamineHCID 67732890HCID 67732890, compound

Product 1

HCID 69228727HCID 69228727, compound

Procedure

Prepared analogously to Example 1b from tert.butyl 4'-[(2-n-propyl-4-methyl-6-phthalimido-1H-benzimidazol-1-yl)-methyl] -biphenyl-2-carboxylate and methylamine.

Sources & evidence

ORD record
ord-74039bcdd7a246339d2084d2ab36e8b9
Source dataset
uspto-grants-1996_05
Patent number
US05521177

Reaction notes

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