HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride → HCID 18347203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Reactant | HCID 18347217 | HCID 18347217 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18347203 | HCID 18347203 | 77.9% |
Reaction Steps
To a solution of 120 mg of the product of Step 3 in 10 mL of CH2Cl2 was added 150 mg of 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride. After stirring for 30 min, the reaction mixture was concentrated in vacuo and purified by silica gel chromatography eluted with 6:1 hexane/EtOAc to give 89 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05521213 |
| Source dataset | uspto-grants-1996_05 |
| ORD ID | ord-2655df9f3a734994bc8263d695aab370 |
| Source note | uspto-grants-1996_05 |