HCID 10324214, compound → HCID 10391723, compound

Participants

Reaction Steps

Using a similar procedure to that described in Example 1, using methanol:dichloromethane (1:99) as the chromatography solvent, 2-(2-oxo-6-phenyl-3-phenylacetylamino-1,2-dihydro-1-pyridyl)-N-(3,3,3-trifluoro-2-hydroxy-1-isopropylpropyl)acetamide was oxidized to afford the title product; HPLC: tR =6.92, FR=2.0, column A, water:acetonitrile (55.45); MS: m/z=514(M+1).

Provenance & Evidence