HCID 10371178, compound → HCID 22405541, compound

Participants

Reaction Steps

2-[3-Benzyloxycarbonylamino-6-(3,5-dimethoxyphenyl)-2-oxo-1,2-dihydro-1-pyridyl]-N-(3,3,3-trifluoro-1-isopropyl-2-oxopropyl)acetamide was subjected to the conditions described in Example 159, except with shaking under a 2.7 bar hydrogen atmosphere, to give the title compound. Chromatography solvent: Dichloromethane:methanol (98:2, 95:5); TLC: Rf =0.35, dichloromethane:methanol (95:5); MS: m/z=456(M+1).

Provenance & Evidence