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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 441292Generated: October 26, 2026

Iodoethane → HCID 54021047, compound

https://huagongshe.com/reaction/441292

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIodoethaneHCID 6340—
ReactantCarbon DisulfideHCID 6348—
Reactant5-Ethylpyridin-2-amineHCID 9812777—
ReactantHCID 86734976HCID 86734976—
SolventAcetonitrileHCID 6342—
SolventTriethylamineHCID 8471—
ProductHCID 54021047HCID 54021047—

Reaction Steps

Following a procedure similar to that described in Example 1 above, 5-ethyl-2-aminopyridine [Ban et al., Chem. Ind. (London) 1964 (17), 710-711] is reacted with carbon disulfide and triethylamine in acetonitrile and the resulting triethylammonium (5-ethyl-2-pyridyl)carbamodithioate rected with ethyl iodide to give ethyl (5-ethyl-2-pyridyl)carbamodithioate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04039550
Source datasetuspto-grants-1977_08
ORD IDord-4d483e6ebdb7428793380a43d6aa3849
Source noteuspto-grants-1977_08