Iodoethane → HCID 54021047, compound

HRID 441292Notes

Reaction equation

HRID 441292 reaction equation
[CH2:1](C1C=CC(N)=NC=1)[CH3:2].C(=S)=S.[CH2:13]([C:15]1[CH:16]=[CH:17][C:18]([NH:21][C:22]([S-:24])=[S:23])=[N:19][CH:20]=1)[CH3:14].C([NH+](CC)CC)C.C(I)C>C(#N)C.C(N(CC)CC)C>[CH2:13]([C:15]1[CH:16]=[CH:17][C:18]([NH:21][C:22]([S:24][CH2:1][CH3:2])=[S:23])=[N:19][CH:20]=1)[CH3:14]

Participants

7

Reactant 4

HCID 6340IodoethaneHCID 6348Carbon DisulfideHCID 98127775-Ethylpyridin-2-amineHCID 86734976HCID 86734976, compound

Product 1

HCID 54021047HCID 54021047, compound

Reagents, catalysts & solvents 2

HCID 6342AcetonitrileSolventHCID 8471TriethylamineSolvent

Procedure

Following a procedure similar to that described in Example 1 above, 5-ethyl-2-aminopyridine [Ban et al., Chem. Ind. (London) 1964 (17), 710-711] is reacted with carbon disulfide and triethylamine in acetonitrile and the resulting triethylammonium (5-ethyl-2-pyridyl)carbamodithioate rected with ethyl iodide to give ethyl (5-ethyl-2-pyridyl)carbamodithioate.

Sources & evidence

ORD record
ord-4d483e6ebdb7428793380a43d6aa3849
Source dataset
uspto-grants-1977_08
Patent number
US04039550

Reaction notes

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